Download PDF by James Morrison (Eds.): Asymmetric Synthesis

By James Morrison (Eds.)

ISBN-10: 0125077017

ISBN-13: 9780125077019

ISBN-10: 032316000X

ISBN-13: 9780323160001

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And Curme, H. G. (1972). In "Physical Methods of Chemistry" (A. Weissberger and B. W. ), Part IIIC, pp. 5 1 - 1 8 1 . Wiley (Interscience), New York. Hoeve, W. , and Wynberg, H. (1980). J. Org. Chem. 45, 2754. Horeau, A. (1969). , p. 3121. Horeau, A. (1977). In "Stereochemistry, Fundamentals and Methods" (H. B. ), Vol. 3, pp. 5 1 - 9 4 . Thieme, Stuttgart. Hudson, C. S. (1909). J. Am. Chem. Soc. 39, 66. , Collet, Α . , and Wilen, S. H. (1981). " Wiley (Interscience), New York. Kauzmann, W. , Walter, J.

And Buckingham, J. (1978). "Atlas of Stereochemistry," 2nd ed. Oxford Univ. Press, New York. Lowry, Τ. M. (1935). " Longmans, Green, London; 2nd ed. (1964), Dover, New York. Lyle, R. , Fribush, Η. , Saavedra, J. , Lyle, G. , and Jacobson, Μ. Κ. (1979). ACS Symp. , No. 101. , and Mosher, H. S. (1964). Biochemistry 3 , 838. Mills, J. A. (1952). J. Chem. Soc, p. 4976. , and Djerassi, C. (1960). J. Am. Chem. Soc. 82, 5247. Pirkle, W. , and Beare, S. D. (1967). J. Am. Chem. Soc 89, 5485. Plattner, PI.

7) gives Cx 2(x + R + 2E) 0 2(x + R) ' (8) If Eq. (8) is written in terms of ee, it becomes Cx 0 2[x + y(\ + ee)] 2[x + j ( l - ee)] * (9) 50 Κ. Κ. A n d e r s e n , D. Μ. Gash, a n d J. D . Robertson There is the possibility of preparing a sample of pure isotopically labeled enantiomer from, for example, a natural product. In this case, assuming as above that the ( + )-enantiomer is prepared, Eq. y/2)(l + ee)] " Equation (9) can be rearranged thus: \_ ee 1/2 (χ + y) - + y) 2 y (11) or (ee) 2 C (x + y) - C x(x + y) 2 = ± 0 yc 2 (12) ± Consider now the situation in which the isolated material is not a racemic modification (a labeled racemic modification is still used as the tracer; Fig.

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Asymmetric Synthesis by James Morrison (Eds.)


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